Determination of lipophilic marine biotoxins in molluscs by. Analyzing pbdes in house dust samples with the tsq quantum. T ptv injection port, provided sample introduction into the tsq quantum. Tsq quantum xls series preinstallation requirements. Triplus is a trademark, and tsq quantum and trace gc ultra are registered tradem arks of thermo fisher scientific inc. Stateoftheart electronics and comprehensive diagnostics are hallmarks of our instruments. The thermo tsq quantum triple quadrupole system performs highly selective reaction monitoringhsrm analyzes complex samples quickly and efficiently.
This tsq quantum ultra getting connected manual provides you with information on how to connect your tsq quantum ultra system. Thermo scientific 7011160863 tsq quantum xls ultra front. This tsq quantum xls series user guide contains a description of the modes of operation and principle hardware components of your tsq quantum xls series system. Tsq quantum ultra getting started version a thermo fisher. Benefits of the tsq quantum ultra include constant neutral loss scanning, parent scanning, highresolution precursor ion selectivity, srm and hsrm in order to deliver a complete solution for the proteomics. Tsq series tsq quantum xls and tsq quantum gc user guide 7011197220 revision b may 2010. Bellagambi, department of chemistry and industrial chemistry, university of pisa, italy claudia p. The thermo scientific tsq quantum access max triple quadrupole mass spectrometer is an ou. Ionbench with the thermo tsq quantum ultra mass spectrometer. Accurate mass data is generated on each of the 25 ions from 168 to 1224 da using the neighboring peaks as internal lock masses. In this table, we compare different tsq triple quadrupole systems in order to showcase which ones are most relevant to your laboratorys needs.
The determination of anabolic steroids in human urine. Regulatory compliance thermo electron san jose performs complete testing and evaluation of its products to. Tsq quantum ultra getting connected includes the following. This preowned thermo tsq quantum ultra lcmsms sensitive triple quad is calibrated to meet oem standards.
Tsq quantum access max triple quadrupole mass spectrometer. Its in beautiful condition and comes to you fully tested, refurbished and in perfect working order. Triple quadrupole lcms thermo fisher scientific us. Thermo scientific tsq quantum xls ultra front replacement cover here is a thermo scientific tsq quantum xls ultra front replacement cover for sale. This device complies with low voltage directive 200695ec and harmonized standard en 610101. The pierce triple quadrupole calibration solution, extended mass range, formulation contains 14 compounds that are ionizable in both positive and negative modes for instrument calibration. Benefits of the tsq quantum ultra include constant neutral loss scanning, parent scanning, highresolution precursor ion selectivity, srm and hsrm in order to deliver a complete solution for the proteomics and large molecule research community. Thermo scientific pierce triple quadrupole calibration. Now available from krss, a used fully refurbished and serviced thermo tsq quantum ultra including thermo surveyor hplc, 3 months warranty, installation and training. We have 1 thermo scientific tsq quantum gc manual available for free pdf download.
Analyzing pbdes in house dust samples with the thermo scientific tsq quantum xls ultra gcmsms in eisrm mode be the first to rate this application. Finnigan tsq quantum ultra am the principle of how accurate mass determinations are made on the tsq quantum ultra am is shown below figure 1. Thermo electron finnigan tsq quantum ultra rensselaer center. The high gain ion detector with accelerating high voltage conversion dynode is set offaxis for noisefree signal detection. Tsq quantum xls ultra gcmsms from thermo scientific. Food safety, environmental, clinical, forensic, toxicology, pharmaceutical and metabolomic sanalyses can all. Tsq quantum ultra emc directive 89336eec as amended by 9231eec and 9368eec emc compliance has been evaluated by u.
The tsq quantum xls gcmsms paired with the trace gc ultra gas chromatograph showed excellent results at low concentrations for the pesticide residues analyzed in the green tea. Thermo scientific tsq quantum xls ultra alturas analytics, inc. Our expert service engineers and chemists can install and custom configure the system to be compliant with the methods you plan to run. Scientific trace gc ultra gas chromatograph, equipped with a backflush valve b. Quantitation of synthetic cannabinoids in urine using a triple stage quadrupole lcms system in forensic toxicology kristine van natta, marta kozak. Faster method development at the highest possible specificity is routinely achievable with the tsq quantum ultra mass spectrometer. Topoccasion thermo tsq quantum ultra lcmsms triple quad. The mass spectrum of azithromycin was obtained utilizing a thermo scientific tsq quantum mass spectrometer systems feature hyperquad quadrupoles. Product specifications with the thermo scientific tsq quantum xls we continue the successful and wellknown tsq triple quadrupole mass spectrometer series, combined with the power, performance and flexibility of the thermo scientific trace gc ultra gas chromatograph. Computer w xcalibur software vacuum pump and all hosing ion max heated electrospray hesi probe. Instructions can be found on the mprophet website and in surinova et al. Quantitative confirmatory analysis of the nida 5 panel. The front window in the ion max ion source housing allows you to.
General chemical state laboratory, pesticide residues laboratory, athens, greece key words tsq quantum ultra surveyor hplc system hsrm food safety pesticide residues. The tsq quantum access max offers several innovative features that provide real benefits. Thermo scientific tsq quantum gc manuals manuals and user guides for thermo scientific tsq quantum gc. Experimental a thermo scientific as 3000 ii autosampler and a thermo scientific trace gc ultra gas chromatograph, equipped with a backflush valve b. Welcome to the thermo electron, finnigan tsq quantum ultra system. The tsq quantum ultra system is available with optional extended mass range emr, accurate mass am, and highfield asymmetric waveform ion mobility spectrometry faims capabilities to meet the demands of the widest range of applications. Tsq quantum triple quadrupole system performs highly selective reaction monitoring hsrm analyzes complex samples quickly and efficiently. The following are registered trademarks in the united states and other countries. Every effort has been made to supply complete and accurate information. The experimental conditions are described in table 1, and the eisrm and nciselected ion monitoring sim parameters are provided in table 2.
For research use only not for use in diagnostic procedures finnigan tsq quantum ultra emr getting started 7011197111 revision a march 2006. Product specifications tsq quantum gc the next evolution. Analysis of microcystins from bluegreen algae using the tsq. Thermo scientific tsq quantum access max specification sheet. Thermo scientific tsq quantum ultra gentech scientific. Technical information contained in this publication is for reference purposes only and is subject to change without notice. The tsq quantum ultra is a member of the tsq family of finnigan mass spectrometers. Tear this sheet from the manual, fold it closed, stamp it, and drop it in the mail. Pdf a new methodology for targeted peptide quantitation in. Determination of lipophilic marine biotoxins in molluscs. Resolution up to 7,500 at mz 508 esi ionization mode. Tsq quantum access max unsurpassed price to performance from the company renowned for innovation in mass spectrometry, the thermo scientific tsq quantum access max is the newest member of the successful tsq product family.
The thermo scientific tsq quantum access is the benchmark triple quadrupole lcmsms for pharmaceutical, environmental, food safety, clinical research, and forensics analysis. Analyzing pbdes in house dust samples with the thermo. Featuring best in class target compound selectivity and analytical performance, the tsq quantum xls ultra is engineered to meet the requirements of the most demanding analytical tasks across food safety, environmental, clinical, forensic, toxicology. This is of significant value when analyzing multiple classes of compounds in one sample that require ionization in both polarities. Op pesticides are the most commonly used insecticides in agriculture and the domestic field. For research use only not for use in diagnostic procedures tsq quantum gc user guide 7011197151 revision a september 2007.
Bch190ne58 vibration dampening one issue that is not addressed by conventional lab furniture for mass spectrometers is the vibration translated by the vacuum pump toward the mass. The determination of anabolic steroids in human urine using. Tsq quantum ultra triple quadrupole mass spectrometer. Ms and msms experiments were performed on a tsq quantum ultra am mass. Thermo scientific tsq quantum ultra mass spectrometer provides ultimate productivity for bioanalytical analysis. The tsq quantum xls delivers unsurpassed performance with superior. View online or download thermo scientific tsq quantum xls ultra user manual. Thermo forma tsq quantum ultra am accurate mass lcmsms. Tsq quantum ultra emc directive 89336eec as amended by 9231eec and 9368eec emc compliance has been evaluated by underwriters laboratories inc. Martins, thermo fisher scientific, barcelona, spain michal godula, thermo fisher scientific, prague, czech republic. Quantitation of synthetic cannabinoids in urine using a. Determination of lipophilic marine biotoxins in molluscs by lcmsms using offline extraction.
The tsq quantum ultra mass spectrometer assures the best available technology for a variety of quantitative applications and the ultimate productivity for bioanalysis. The ms analysis was performed with electrospray ionization esi interface in both negative and positive ion modes. This tsq quantum access was built in 20082009 truly like new. Tsq quantum xls ultra gc msms from thermo scientific.
Tsq quantum xls ultra triple quadrupole gcms 8 the tsq quantum xls ultra triple quadrupole mass spectrometer addresses the requirements of the most demanding analytical tasks across applications. Thermo scientific tsq quantum xls user manual pdf download. With the thermo scientific tsq quantum xls we continue the successful and wellknown tsq triple quadrupole mass spectrometer series, combined with the power, performance and flexibility of the thermo scientific trace gc ultra gas chromatograph. Quantitative confirmatory analysis of the nida 5 panel using. Thermo scientific finnigan tsq quantum ultra mass spectrometer featuring the proprietary thermo scientific hyperquad quadrupole mass analyzer system and provides ultimate productivity for bioanalytical analysis. Bch190ne58 detailed techniccal specifications noise enclosure for vacuum pumps noise reduction performance. The thermo scientific tsq quantum xls ultra gcmsms system, run in both ei and nci modes, was used for analysis.
This tsq quantum ultra getting started manual provides you with information on how to set up, calibrate, and tune the tsq quantum ultra tsq quantum ultra. Thermo tsq quantum ultra lcmsms multiplexing system. T ptv injection port, thermo scientific trace gc ultra provided sample introduction into the tsq quantum xls mass spectrometer. Thermo fisher scientific, san jose, ca application note. Finnigan tsq quantum ultra thermo fisher scientific. Acephate ap, methamidophos mmp, omethoate omet and dimethoate dmet are organophosphorus pesticides ops pesticides. This system features the innovative qedmsms scan mode for unmatched sensitivity and selectivity. Abdelgalil, in profiles of drug substances, excipients and related methodology, 2014. Tsq quantum ultra ion max source introduced 1986 tsq 70 first fully computercontrolled tsq with hyperbolic quadrupoles 2005 tsq quantum ultra hesi introduced 1997 tsq 7000 api 2 interface 2000 tsq quantum first commercially available triple stage quadrupole with hsrm 0. The formulation has been specifically optimized for use with the tsq endura series and tsq quantiva series instruments. Overview to scale the picture below is a simulation at scale of the thermo tsq quantum ultra lcms system mass spectrometer system right side connected with a dionex uhplc left side, installed on a ionbench ms mass spec bench or table.
Benefits of the tsq quantum ultra include constant neutral loss scanning, parent scanning, highresolution precursor ion selectivity. Tsq quantum xls, tsq quantum gc, and trace gc ultra. It features the revolutionary product specifications thermo scienti. Jul 31, 2019 tsq quantum triple quadrupole system performs highly selective reaction monitoring hsrm analyzes complex samples quickly and efficiently. Determination of lipophilic marine biotoxins in molluscs by lcmsms using offline extraction francesca g. Find pricing on new and used thermo tsq quantum ultras and other mass spectrometers. Applications such as pharmaceutical development, environmental and food safety testing, clinical research, and forensic toxicology demand analytical sensitivity and specificityeven when budgets are constrained. Infusion of a mixture of polyethylene glycols pegs of average molecular weights 200,400, 600, and at 50 pmoles.
Thermo scientific tsq quantum xls ultra pdf user manuals. Switching the ionization mode from ei to nci on the. Tsq quantum gc the next evolution in gcmsms systems the thermo scientific tsq quantum gc defines a new standard of excellence in gcmsms for environmental food safety, pharmaceutical, and clinical research laboratories. Thermo electron finnigan tsq quantum ultra rensselaer. It is ideal for determination of masses in complex mixtures and quantitative analyses. Regulatory compliance thermo electron san jose performs complete testing and evaluation of its. Low voltage safety compliance this device complies with low voltage directive 7323eec and harmonized standard en 610101. Triple quadrupole lcms system product comparison different applications require different levels of system sensitivity, resolution, and speed. In this table, we compare different tsq triple quadrupole systems in order to showcase which ones are most relevant to.
Ultra gcmsms is specially suited for multi component trace analysis in on run, and is already prepared for fastgc applications on. L produces 27 ammoniated peg ions from 124 to 1268 da. Diese srm wurden wie zuvor beschrieben durch eigene tuneexperimente an einem tsq quantum ultra thermofisher ermittelt oder aus. Analysis of microcystins from bluegreen algae using the tsq quantum ultra lcmsms system be the first to rate this. Switchable between gcms and lcms mass range up to mz3000 scan speeds. Using the instruments srm functionality allows the user to identify, confirm, and quantify at a wide range of concentrations in one analytical run. The thermo scientific tsq quantum xls ultra is the new gold standard in gcmsms.